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Carbon-coated nickel nanoparticles that make CO from CO2

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N-doped carbon plus a carbon coat lets metallic Ni nanoparticles reach about 94% CO faradaic efficiency, suppressing hydrogen evolution.

Source

Carbon-supported Ni nanoparticles for efficient CO<sub>2</sub> electroreduction

Jia M, Choi C, Choi C, et al. · Chemical science · 2018

doi.org/10.1039/c8sc03732aRead the full paper ↗61 citationscc by

Study at a glance

Design
Other — Pyrolyzed carbon-supported Ni nanoparticles for aqueous CO2-to-CO electrolysis with DFT
N
Electrocatalysis materials study — no sample N
Population
Ni nanoparticle catalysts on N-doped carbon supports
Outcome
CO faradaic efficiency and current density in CO2 electroreduction

Structured fields used in claim comparison tables when every cited study has a complete layer.

What they did

Authors pyrolyzed Ni with organic linkers and carbon black, characterized Ni loading (~3.6–4.0 wt%), XPS (Ni0, no Ni–N single-atom peak), HAADF-STEM (10–100 nm particles), and measured aqueous CO2-to-CO electrolysis plus DFT.

What they found

CO FE up to ~94% at −0.7 V vs RHE and 22.7 mA cm−2 at −1.1 V. Carbon coating plus N-doped support suppress HER. XPS/STEM argue metallic nanoparticles, not Ni single atoms or nitride.

The limits

What it doesn't show

Long-term industrial MEA stacks and C2+ products are not claimed; performance is compared to prior Ni catalysts, not a full techno-economic plant.

Key terms

Faradaic efficiency (FE)
Fraction of current that produces CO rather than H2.
HER suppression
Carbon coat/N-support that make H2 evolution less competitive.
Ni0 nanoparticles
Metallic nickel particles 10–100 nm, not isolated Ni–N4 sites.
N-doped carbon
Support with pyridinic/pyrrolic/graphitic nitrogen.
CO2-to-CO
Two-electron electroreduction to carbon monoxide.

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Peak CO FE is about:

Common questions

Best CO FE?

About 94% at −0.7 V vs RHE.

Current density cited?

22.7 mA cm−2 at −1.1 V.

Single atoms?

No: STEM 10–100 nm particles; no Ni–N XPS peak.

Ni loading?

~3.6–4.0 wt%.

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