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Ultrathin porous CoP nanosheets drive HER

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Phosphidation of Co3O4 yields sub-1.1 nm porous CoP sheets with exposed {200} facets and high HER mass activity.

Source

Sub-1.1 nm ultrathin porous CoP nanosheets with dominant reactive {200} facets: a high mass activity and efficient electrocatalyst for the hydrogen evolution reaction

Zhang C, Huang Y, Yu Y, et al. · Chemical science · 2017

doi.org/10.1039/c6sc05687cRead the full paper ↗88 citationscc by

Study at a glance

Design
Other — Ultrathin porous CoP nanosheets for acidic HER with DFT H-adsorption analysis
N
Electrocatalysis materials study — no sample N
Population
CoP ultrathin porous nanosheet electrodes in 0.5 M H2SO4
Outcome
HER overpotential, Tafel slope, and mass activity

Structured fields used in claim comparison tables when every cited study has a complete layer.

What they did

Authors converted Co3O4 to CoP ultrathin porous nanosheets, measured HER in 0.5 M H2SO4, extracted capacitance/ECSA, and computed H adsorption on CoP(100).

What they found

56 and 131 mV reach 10 and 100 mA cm–2; Tafel slope 44 mV dec–1; mass activity 151 A g–1 at 100 mV; ~100% Faradaic efficiency and 20 h stability. P-terminated (200) is preferred.

The limits

What it doesn't show

Device-scale alkaline or seawater HER is untested; ECSA uses an assumed 40 μF cm–2 specific capacitance.

Key terms

HER
Hydrogen evolution reaction: 2H+ + 2e– → H2.
Tafel slope
mV per decade of current; encodes the rate-determining electron-transfer steps.
Mass activity
Current per gram of catalyst at a stated overpotential.
{200} facet
Preferentially exposed CoP plane; P-termination is computed more stable.
Faradaic efficiency
Fraction of charge that produces the intended product (here H2).

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CoP UPNSs are made by:

Common questions

How are CoP UPNSs made?

Low-temperature phosphidation of Co3O4 with NaH2PO2.

What overpotential gives 10 mA cm–2?

56 mV.

What is the mass activity at 100 mV?

151 A g–1.

Which termination is more stable?

P-terminated CoP(200)/ (100).

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