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Does chemical fixation squash the living cortex?

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In adult mouse barrel cortex, aldehyde perfusion shrank tissue ~30% and left only 2.5% extracellular space versus 15.4% after high-pressure freezing; cryo tissue also had smaller astrocyte volume, looser glial coverage, and more docked vesicles.

Source

Ultrastructural analysis of adult mouse neocortex comparing aldehyde perfusion with cryo fixation

Korogod N, Petersen CC, Knott GW · eLife · 2015

doi.org/10.7554/elife.05793Read the full paper ↗335 citationscc by

Study at a glance

Design
Animal / in-vitro — Quantitative EM comparison of adult mouse somatosensory neocortex after aldehyde perfusion versus high-pressure freezing/freeze substitution
N
N=4 · Primary neuropil comparisons N=4 mice per fixation; cortical thickness used N=6 fresh vs 14 chemically fixed; vessel coverage n=11 cryo vs 69 perfused
Population
Adult C57BL/6 mice (7–10 weeks), primary somatosensory barrel cortex
Outcome
Tissue shrinkage, extracellular-space and astrocyte volume fractions, synapse density/coverage, vesicle shape and docking

Structured fields used in claim comparison tables when every cited study has a complete layer.

What they did

Compared fresh vs chemically fixed cortical thickness, then serial-section EM of high-pressure-frozen vs aldehyde-perfused neuropil (N=4 mice/group), scoring ECS, astrocyte/neurite volumes, synapse density, perisynaptic gaps, astrocytic coverage of synapses and capillaries, and vesicle geometry.

What they found

Cortical thickness −16%; ~30% volume loss. ECS 15.4 ± 5.4% cryo vs 2.47 ± 1.5% chemical (p=0.003). Astrocyte volume 7.4% vs 14.4% (p=0.01). Synapse density 0.63 vs 0.87 µm⁻³ (p=0.042). Perisynaptic gap 166 vs 53 nm. Capillary astrocyte coverage 63% vs 94%. Cryo revealed more docked vesicles; flattened ‘type 2’ vesicles were a chemical-fixation artifact.

The limits

What it doesn't show

High-pressure freezing still samples tiny freshly cut pieces, so it is not a whole-brain connectomics method; ‘more native’ does not prove every cryo number matches living cortex under all conditions.

Key terms

High-pressure freezing
Cryo fixation that vitrifies small tissue with liquid nitrogen at high pressure to avoid ice crystals.
Extracellular space (ECS)
Watery volume between cells; ~15% after cryo vs ~2.5% after aldehydes here.
Astrocytic endfeet
Glial processes around capillaries; coverage looked nearly complete after chemicals but only ~63% after cryo.
Docked vesicles
Synaptic vesicles against the presynaptic membrane, ready for release; more numerous after cryo fixation.
Type 1 vs type 2 synapses
Gray’s EM classes; flattened vesicles of ‘type 2’ appeared only after chemical fixation.
Freeze substitution
Low-temperature dehydration/embedding of frozen tissue for EM.

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Cryo vs chemical ECS:

Common questions

ECS after cryo vs chemicals?

15.4% vs 2.47% (six-fold).

How much did cortex shrink?

About 16% thickness, ~30% volume.

Astrocyte volume?

7.4% cryo vs 14.4% chemical.

Capillary glial coverage?

62.9% cryo vs 94.4% chemical.

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