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Green chemistry

Ten-gram grinding makes lanthanum coordination polymers

Zhang L, Shi H, Tan X, et al. · Frontiers in chemistry · 2022

Open access · cc by · source: Europe PMC

Manual grinding of LaCl3 with 5-sulfosalicylate and 8-hydroxyquinoline yields ternary CPs whose IR/XPS/MS match a chelated nanocomposite.

Key findings

ESI-MS 912.6347 g mol–1; COO IR bands shift on La chelation; XPS shows N–La and O–S; BET 5.58 m2 g–1 mesopores. Solution-phase LCP-3 has different UV/IR, proving method-dependent nanostructures.

Methodology

Authors ground 5-SSA, 8-hq and LaCl3·7H2O for 1 h at 25 °C, compared a solution-phase analogue, and characterized products by NMR, ESI-MS, XPS, XRD, BET and TG.

Limitations

No single-crystal structure of LCP-1; antibacterial/antitumor assays are cellular screens, not a molecular MIC mechanism.

How this study connects

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