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Polymers

Soft polymers wet UiO-66 without interfacial voids

Semino R, Moreton JC, Ramsahye NA, et al. · Chemical science · 2018

Open access · cc by · source: Europe PMC

MD shows flexible PVDF and PEG fill UiO-66 surface pockets; rigid PIM-1 and PS leave microvoids and fail as 70 wt% films.

Key findings

PIM-1/PS interfaces have microvoids (up to 13 Å and 8 Å) and long recovery distances (z-length A 15 and 9 Å). PVDF and PEG show no voids, chain-end pore penetration, and H-bonds at 2.0 vs 1.7 Å. PEG Young's modulus more than doubles at 70 wt% MOF, but N2 area collapses; PVDF keeps MOF porosity.

Methodology

Authors built a hydrated {101} UiO-66 slab, equilibrated PIM-1, PS, PVDF and PEG against it, and made 70–80 wt% PEG MMMs compared with PVDF, PS and PIM-1 films.

Limitations

No gas-separation permeance on the new PEG MMMs; PEG pore blocking is inferred from BET, not in situ pore tomography; only one MOF topology was modelled.

How this study connects

Role on claims

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  • SupportsPolymersconcept

    MD shows flexible PVDF and PEG fill UiO-66 surface pockets; rigid PIM-1 and PS leave microvoids and fail as 70 wt% films.

    Evidence for the claim as stated.

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